8-[acetyl(phenyl)amino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N²-[(dimethylamino)methylene]guanosine

Base Information

• Chemical Name: 8-[acetyl(phenyl)amino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N²-[(dimethylamino)methylene]guanosine
• CAS No.: 1426845-81-9
• Molecular Formula: C₄₂H₄₃N₇O₇
• Molecular Weight: 757.846

Synonyms:8-[acetyl(phenyl)amino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N²-[(dimethylamino)methylene]guanosine

Chemical Property of 8-[acetyl(phenyl)amino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N²-[(dimethylamino)methylene]guanosine

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Technology Process of 8-[acetyl(phenyl)amino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N²-[(dimethylamino)methylene]guanosine

There total 1 articles about 8-[acetyl(phenyl)amino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N²-[(dimethylamino)methylene]guanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

8-[acetyl(phenyl)amino]-2'-deoxy-N2-[(dimethylamino)methylene]guanosine (1426845-72-8) + 4,4'-dimethoxytrityl chloride (40615-36-9) → 8-[acetyl(phenyl)amino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N2-[(dimethylamino)methylene]guanosine (1426845-81-9)

Guidance literature:

With pyridine; at 20 ℃; for 16h;

DOI:10.1055/s-2007-990913

Reference yield: 68.0%

8-[acetyl(phenyl)amino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N2-[(dimethylamino)methylene]guanosine (1426845-81-9) + N,N,N',N'-tetraisopropyl 2-cyanoethylphosphorodiamidite (102691-36-1) → 8-[acetyl(phenyl)amino]-3'-O-[(2-cyanoethyloxy)(diisopropylamino)phosphino]-2'-deoxy-5'-O-(4,4'-dimethoxytrityl)-N2-[(dimethylamino)methylene]guanosine

Guidance literature:

With dichloroisoproterenol; In tetrahydrofuran; dichloromethane; acetonitrile; at 20 ℃; for 1h;

DOI:10.1055/s-2007-990913

upstream raw materials:

8-[acetyl(phenyl)amino]-2'-deoxy-N²-[(dimethylamino)methylene]guanosine

4,4'-dimethoxytrityl chloride

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