2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine

Base Information

Chemical Name:2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine
CAS No.:131136-43-1
Molecular Formula:C₂₀H₂₈N₂O₂
Molecular Weight:328.455
Hs Code.:

Synonyms:2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine

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Technology Process of 2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine

There total 6 articles about 2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 100-39-0
benzyl bromide

: 131136-32-8
2-hydroxy-3,6-diisobutyl-5-methoxypyrazine

: 131136-43-1
2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine

Guidance literature:: With potassium hydroxide; tetramethylammonium bromide; In chloroform; at 30 ℃; for 36h; Irradiation;
DOI:10.3987/COM-90-5364

Reference yield:

: 19803-49-7
3-chloro-2,5-bis(2-methylpropyl)pyrazine

: 131136-43-1
2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine

Guidance literature:: Multi-step reaction with 5 steps

1: 95 percent / methanol / 3 h / Heating

2: 90 percent / 60percent H₂O₂, maleic anhydride / CHCl₃ / 12 h / Ambient temperature

3: 73 percent / 1.5 h / Heating

4: 99 percent / 10percent K₂CO₃ / methanol / 0.5 h / Heating

5: 80 percent / 10percent KOH, Me₄NBr / CHCl₃ / 36 h / 30 °C / Irradiation

With maleic anhydride; potassium hydroxide; dihydrogen peroxide; tetramethylammonium bromide; potassium carbonate; In methanol; chloroform;
DOI:10.3987/COM-90-5364

Reference yield:

: 19803-48-6
2-chloro-3,6-diisobutylpyrazine 4-oxide

: 131136-43-1
2-benzyloxy-3,6-diisobutyl-5-methoxypyrazine

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / methanol / 3 h / Heating

2: 73 percent / 1.5 h / Heating

3: 99 percent / 10percent K₂CO₃ / methanol / 0.5 h / Heating

4: 80 percent / 10percent KOH, Me₄NBr / CHCl₃ / 36 h / 30 °C / Irradiation

With potassium hydroxide; tetramethylammonium bromide; potassium carbonate; In methanol; chloroform;
DOI:10.3987/COM-90-5364