Technology Process of C28H37N5O4S*ClH
There total 8 articles about C28H37N5O4S*ClH which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
1,4-dioxane;
at 20 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / tetrahydrofuran / 24 h
2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / -60 °C / Inert atmosphere
2.2: 1 h / -60 °C
2.3: -60 °C
3.1: potassium fluoride / N,N-dimethyl-formamide
4.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
With
4-methyl-morpholine; hydrogenchloride; potassium fluoride; copper(l) iodide; N-ethyl-N,N-diisopropylamine; isobutyl chloroformate;
In
tetrahydrofuran; 1,4-dioxane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate; imidazole-1-sulfonyl azide hydrochloride / copper(ll) sulfate pentahydrate / methanol
2.1: N-ethyl-N,N-diisopropylamine; copper(l) iodide / tetrahydrofuran / 24 h
3.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / -60 °C / Inert atmosphere
3.2: 1 h / -60 °C
3.3: -60 °C
4.1: potassium fluoride / N,N-dimethyl-formamide
5.1: hydrogenchloride / 1,4-dioxane / 2 h / 20 °C
With
4-methyl-morpholine; hydrogenchloride; imidazole-1-sulfonyl azide hydrochloride; potassium fluoride; copper(l) iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine; isobutyl chloroformate;
copper(ll) sulfate pentahydrate;
In
tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
