(2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone

Base Information

Chemical Name:(2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone
CAS No.:210291-41-1
Molecular Formula:C₁₉H₃₈O₂Si
Molecular Weight:326.595
Hs Code.:

Synonyms:(2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone

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Chemical Property of (2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone

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Technology Process of (2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone

There total 1 articles about (2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 69739-34-0
t-butyldimethylsiyl triflate

: 201230-42-4
(1'R,2R,3R,6R)-2-(1'-hydroxypropyl)-6-isopropyl-3-methylcyclohexanone

: 210291-41-1
(2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone

Guidance literature:: With pyridine; dmap; Ambient temperature;
DOI:10.1016/S0957-4166(98)00013-5

Reference yield: 98.0%

: 210291-41-1
(2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone

: 210291-44-4
(1S,2S,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanol

Guidance literature:: With sodium tetrahydroborate; In methanol; for 2h; Ambient temperature;
DOI:10.1016/S0957-4166(98)00013-5

Reference yield:

: 210291-41-1
(2R,3R,6R)-2-[(R)-1-(tert-Butyl-dimethyl-silanyloxy)-propyl]-6-isopropyl-3-methyl-cyclohexanone

: 210291-39-7
(1'R,1S,2R,3R,6R)-2-(1'-hydroxypropyl)-6-isopropyl-3-methylcyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / NaBH₄ / methanol / 2 h / Ambient temperature

2: 94 percent / tetra-butyl ammonium fluoride / tetrahydrofuran / 3 h / Ambient temperature

With sodium tetrahydroborate; tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol;
DOI:10.1016/S0957-4166(98)00013-5