[3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol

Base Information

• Chemical Name: [3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol
• CAS No.: 193278-20-5
• Molecular Formula: C₂₂H₂₉N₇O₇S
• Molecular Weight: 535.581

Synonyms:[3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol

Chemical Property of [3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol

Chemical Property:

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Technology Process of [3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol

There total 1 articles about [3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

Ng-nitroargininal ethyl cyclol hydrochloride (180250-77-5) + [3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetic acid (179523-53-6) → [3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol (193278-20-5)

Guidance literature:

With 4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In acetonitrile;

DOI:10.1016/S0960-894X(97)00258-8

Reference yield: 85.0%

acetic acid (64-19-7,77671-22-8) + [3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol (193278-20-5) → [3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-L-argininal ethyl cyclol, acetate salt

Guidance literature:

With hydrogen; palladium 10% on activated carbon; In ethanol; water; for 44h; under 1034.32 - 1292.9 Torr;

Reference yield:

[3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetyl-Ng-nitro-L-argininal ethyl cyclol (193278-20-5) → N-((S)-1-Carbamimidoyl-2-ethoxy-piperidin-3-yl)-2-(2-oxo-3-phenylmethanesulfonylamino-2H-pyridin-1-yl)-acetamide (195204-06-9)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethanol; water; acetic acid;

DOI:10.1016/S0960-894X(97)00258-8

upstream raw materials:

Ng-nitroargininal ethyl cyclol hydrochloride

[3-[(benzylsulfonyl)amino]-2-oxo-1,2-dihydropyridyl]acetic acid

Downstream raw materials:

N-((S)-1-Carbamimidoyl-2-ethoxy-piperidin-3-yl)-2-(2-oxo-3-phenylmethanesulfonylamino-2H-pyridin-1-yl)-acetamide

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