ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate

Base Information

Chemical Name:ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate
CAS No.:175886-23-4
Molecular Formula:C₂₁H₂₂O₄
Molecular Weight:338.403
Hs Code.:

Synonyms:ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate

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Technology Process of ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate

There total 1 articles about ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1077-68-5
4-hydroxy-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-one

: 2882-19-1,2216-90-2
ethyl 2-phenyl-2-bromoacetate

: 175886-23-4
ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate

Guidance literature:: With potassium phosphate; In dimethyl sulfoxide; at 20 ℃; for 2h;
DOI:10.1002/jhet.5570330124

Reference yield: 56.0%

: 175886-23-4
ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate

: 133601-20-4
2-phenyl-3,4,5,6-tetrahydrocycloheptabenzofuran

: (1R,9aS)-9a-Hydroxy-1-phenyl-1,6,7,8,9,9a-hexahydro-2-oxa-benzo[cd]azulene-1-carboxylic acid ethyl ester

Guidance literature:: In acetonitrile; for 1.5h; Irradiation;
DOI:10.1002/jhet.5570330124

Reference yield: 43.0%

: 175886-23-4
ethyl 2-(5-oxo-6,7,8,9-tetrahydro-5H-benzocyclohepten-4-yloxy)phenylacetate

: (1R,9aR)-9a-Hydroxy-1-phenyl-1,6,7,8,9,9a-hexahydro-2-oxa-benzo[cd]azulene-1-carboxylic acid ethyl ester

: (1R,9aS)-9a-Hydroxy-1-phenyl-1,6,7,8,9,9a-hexahydro-2-oxa-benzo[cd]azulene-1-carboxylic acid ethyl ester

Guidance literature:: With potassium phosphate; ethyl 2-phenyl-2-bromoacetate; In dimethyl sulfoxide; at 60 ℃; for 1h;
DOI:10.1002/jhet.5570330124