benzyl [cyano-¹⁴C] cyanide

Base Information

• Chemical Name: benzyl [cyano-¹⁴C] cyanide
• CAS No.: 4701-32-0
• Molecular Formula: C₈H₇N
• Molecular Weight: 119.139
• Mol file: 4701-32-0.mol

Synonyms:benzyl [cyano-¹⁴C] cyanide

Chemical Property of benzyl [cyano-¹⁴C] cyanide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzyl [cyano-¹⁴C] cyanide

There total 6 articles about benzyl [cyano-¹⁴C] cyanide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

sodium 14C-cyanide (3396-82-5) + benzyl chloride (100-44-7) → benzyl [cyano-14C] cyanide (4701-32-0)

Guidance literature:

With tetrabutylammomium bromide; In ethanol; water; for 6.5h; Heating;

DOI:10.1002/jlcr.450

Reference yield:

potassium [14C]cyanide + benzyl chloride (100-44-7) → benzyl [cyano-14C] cyanide (4701-32-0)

Guidance literature:

With sodium iodide; In acetone; for 20h; Reflux; Sealed tube;

DOI:10.1002/jlcr.3382

Reference yield:

[14C]potassium cyanide (5373-08-0) + benzyl bromide (100-39-0) → benzyl [cyano-14C] cyanide (4701-32-0)

Guidance literature:

With tetrabutylammomium bromide; In water; for 0.0666667h; microwave irradiation;

DOI:10.1002/jlcr.1078

upstream raw materials:

[14C]potassium cyanide

benzyl chloride

sodium 14C-cyanide

benzyl bromide

Downstream raw materials:

(RS)-[1-14C]-α-methylbenzyl cyanide

2-phenyl[1-¹⁴C]acetic acid

Toluol-p-sulfonsaeure-2-phenyl-<1-¹⁴C>ethylester

2-phenyl[1-¹⁴C]ethanol