C₂₇H₂₃OP

Base Information

• Chemical Name: C₂₇H₂₃OP
• CAS No.: 1310801-12-7
• Molecular Formula: C₂₇H₂₃OP
• Molecular Weight: 394.453
• Mol file: 1310801-12-7.mol

Synonyms:C₂₇H₂₃OP

Chemical Property of C₂₇H₂₃OP

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₇H₂₃OP

There total 2 articles about C₂₇H₂₃OP which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzalacetophenone (94-41-7) + diphenylphosphane (829-85-6) → (S)-Ph2PCH(Ph)CH2COPh (1244964-81-5) + C27H23OP (1310801-12-7)

Guidance literature:

With C₁₅H₂₄ClCuN₂O₂; In tetrahydrofuran; at -20 ℃; for 3h; Temperature; Solvent; enantioselective reaction;

DOI:10.1016/j.tetlet.2013.10.158

Reference yield:

diphenylphosphane (829-85-6) + 1,3-diphenyl-propen-3-one (614-47-1) → (S)-Ph2PCH(Ph)CH2COPh (1244964-81-5) + C27H23OP (1310801-12-7)

Guidance literature:

diphenylphosphane; With 2,6-bis((S,S)-1-p-tolyl-4,5-diphenyl-4,5-dihydro-1H-imidazol-2-yl)phenylpalladium(II) bromide; potassium acetate; In toluene; for 0.5h; Inert atmosphere; Schlenk technique;

1,3-diphenyl-propen-3-one; In toluene; at 0 ℃; for 12h; enantioselective reaction; Inert atmosphere; Schlenk technique;

DOI:10.1021/om500144b

upstream raw materials:

benzalacetophenone

diphenylphosphane

1,3-diphenyl-propen-3-one