phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside

Base Information

Chemical Name:phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside
CAS No.:261926-71-0
Molecular Formula:C₄₉H₅₀O₁₀S
Molecular Weight:830.996
Hs Code.:

Synonyms:phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside

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Chemical Property of phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside

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Technology Process of phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside

There total 7 articles about phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₆₃H₆₂O₁₆S₃

: 261926-71-0
phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside

Guidance literature:: With sodium tetrahydroborate; In N,N-dimethyl-formamide; at 70 ℃;
DOI:10.1016/S0040-4039(00)00427-5

Reference yield:

: 98-88-4
benzoyl chloride

: 261926-71-0
phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: NaBH₄ / dimethylformamide / 70 °C

With pyridine; sodium tetrahydroborate; In N,N-dimethyl-formamide; 1: Esterification / 2: Hydrogenolysis;
DOI:10.1016/S0040-4039(00)00427-5

Reference yield:

: 287945-03-3
C₃₅H₃₈O₁₀S

: 261926-71-0
phenyl 3'-O-allyl-2,2'-di-O-benzoyl-4,4'-di-O-benzyl-6,6'-dideoxy-1-thio-β-D-laminaribioside

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / BF₃*OEt₂; Me₂NH*BH₃ / CH₂Cl₂

2: pyridine

3: pyridine

4: NaBH₄ / dimethylformamide / 70 °C

With pyridine; sodium tetrahydroborate; dimethylamine borane; boron trifluoride diethyl etherate; In dichloromethane; N,N-dimethyl-formamide; 1: Ring cleavage / 2: Tosylation / 3: Esterification / 4: Hydrogenolysis;
DOI:10.1016/S0040-4039(00)00427-5