4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate

Base Information

Chemical Name:4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate
CAS No.:1093111-57-9
Molecular Formula:C₄H₆O₄*C₁₈H₂₁NS
Molecular Weight:401.527
Hs Code.:

Synonyms:4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate

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Chemical Property of 4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate

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Technology Process of 4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate

There total 7 articles about 4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 508233-95-2
4-[2-(4-methylphenylsulfanyl)phenyl]piperidine

: 110-15-6
succinic acid

: 1093111-57-9
4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate

Guidance literature:: In ethyl acetate;

Reference yield:

: 106-45-6
para-thiocresol

: 1093111-57-9
4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium tert-butylate / 1-methyl-pyrrolidin-2-one / 2 - 3 h / 70 - 120 °C

2.1: n-butyllithium / hexane; n-heptane / 1.17 h / 20 °C

2.2: -40 °C

2.3: 0 - 10 °C

3.1: triethylsilane; trifluoroacetic acid / 18 h / 50 - 60 °C

4.1: hydrogen bromide; acetic acid / 18 h / 45 - 80 °C

5.1: sodium hydroxide; water / ethyl acetate / 0.25 h / pH 13 - 14

6.1: ethyl acetate

With triethylsilane; sodium hydroxide; n-butyllithium; potassium tert-butylate; water; hydrogen bromide; acetic acid; trifluoroacetic acid; In 1-methyl-pyrrolidin-2-one; hexane; n-heptane; ethyl acetate;

Reference yield:

: 15861-49-1
1-bromo-2-(4-methylphenylsulfanyl)benzene

: 1093111-57-9
4-(2-(4-tolylsulfanyl)phenyl)piperidin monosuccinate

Guidance literature:: Multi-step reaction with 5 steps

1.1: n-butyllithium / hexane; n-heptane / 1.17 h / 20 °C

1.2: -40 °C

1.3: 0 - 10 °C

2.1: triethylsilane; trifluoroacetic acid / 18 h / 50 - 60 °C

3.1: hydrogen bromide; acetic acid / 18 h / 45 - 80 °C

4.1: sodium hydroxide; water / ethyl acetate / 0.25 h / pH 13 - 14

5.1: ethyl acetate

With triethylsilane; sodium hydroxide; n-butyllithium; water; hydrogen bromide; acetic acid; trifluoroacetic acid; In hexane; n-heptane; ethyl acetate;