Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester

Base Information

Chemical Name:Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester
CAS No.:115522-54-8
Molecular Formula:C₁₅H₂₃NO₅S₂
Molecular Weight:361.483
Hs Code.:

Synonyms:Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester

Suppliers and Price of Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester

There total 5 articles about Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 115522-50-4,115522-52-6
N-((1R,4R)-4-Hydroxy-cycloheptyl)-4-methyl-benzenesulfonamide

: 124-63-0
methanesulfonyl chloride

: 115522-54-8
Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1016/S0040-4039(00)95578-3

Reference yield:

: 876938-53-3
Cyclohepta-1,3-diene

: 115522-54-8
Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: 71 percent / LiCl, p-benzoquinone / Pd(OAc)2 (7percent) / acetic acid

2: 70 percent / acetonitrile; dimethylsulfoxide / 3 h / 80 °C

3: 94 percent / H₂ / RhCl(PPh₃)3 / ethanol / 20 h / 20 °C / 4560 Torr

4: 97 percent / NaOH / methanol; H₂O

5: 98 percent / Et₃N / tetrahydrofuran

With sodium hydroxide; hydrogen; triethylamine; p-benzoquinone; lithium chloride; palladium diacetate; RhCl(PPh₃)3; In tetrahydrofuran; methanol; ethanol; water; acetic acid; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/S0040-4039(00)95578-3

Reference yield:

: 82736-40-1
(Z)-1-acetoxy-4-chlorocyclohept-2-ene

: 115522-54-8
Methanesulfonic acid (1R,4R)-4-(toluene-4-sulfonylamino)-cycloheptyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / acetonitrile; dimethylsulfoxide / 3 h / 80 °C

2: 94 percent / H₂ / RhCl(PPh₃)3 / ethanol / 20 h / 20 °C / 4560 Torr

3: 97 percent / NaOH / methanol; H₂O

4: 98 percent / Et₃N / tetrahydrofuran

With sodium hydroxide; hydrogen; triethylamine; RhCl(PPh₃)3; In tetrahydrofuran; methanol; ethanol; water; dimethyl sulfoxide; acetonitrile;
DOI:10.1016/S0040-4039(00)95578-3