Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester

Base Information

Chemical Name:Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester
CAS No.:148014-89-5
Molecular Formula:C₇₈H₇₄O₁₆
Molecular Weight:1267.44
Hs Code.:

Synonyms:Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester

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Chemical Property of Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester

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Technology Process of Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester

There total 6 articles about Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 148014-36-2
4-Benzyloxy-2-methoxy-3,5,6-trimethyl-benzoyl chloride

: 148014-89-5
Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

2: H₂ / Pd/C / methanol; ethyl acetate

3: ethyl acetate / Ambient temperature

4: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With n-butyllithium; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm960437a

Reference yield:

: 4-Benzyloxy-2-methoxy-3,5,6-trimethyl-benzoic acid

: 148014-89-5
Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester

Guidance literature:: Multi-step reaction with 5 steps

1: oxalyl chloride / CH₂Cl₂ / a) RT, 30 min, b) reflux, 30 min

2: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

3: H₂ / Pd/C / methanol; ethyl acetate

4: ethyl acetate / Ambient temperature

5: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With n-butyllithium; oxalyl dichloride; hydrogen; palladium on activated charcoal; In methanol; dichloromethane; ethyl acetate;
DOI:10.1021/jm960437a

Reference yield:

: 148014-38-4
C₄₂H₄₂O₇

: 148014-89-5
Isophthalic acid bis-[4-(4-benzhydryloxycarbonyl-3-methoxy-2,5,6-trimethyl-phenoxycarbonyl)-3-methoxy-2,5,6-trimethyl-phenyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / Pd/C / methanol; ethyl acetate

2: ethyl acetate / Ambient temperature

3: 1.) n-BuLi / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, from -78 deg C, 10 min to RT, overnight

With n-butyllithium; hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm960437a