(2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene

Base Information

Chemical Name:(2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene
CAS No.:85363-50-4
Molecular Formula:C₁₆H₁₈P
Molecular Weight:241.293
Hs Code.:

Synonyms:(2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene

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Chemical Property of (2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene

Chemical Property:

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Technology Process of (2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene

There total 3 articles about (2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 43625-65-6
trimethyloxonium cation

: 85363-47-9
(2Z,4Z,6Z)-9-Benzyl-9-phospha-bicyclo[6.1.0]nona-2,4,6-triene

: 85363-50-4
(2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene

Guidance literature:: DOI:10.1016/S0040-4039(00)85746-9

Reference yield:

: 4545-85-1
benzyldichlorophosphane

: 85363-50-4
(2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / diethyl ether / -78 °C

In diethyl ether;
DOI:10.1016/S0040-4039(00)85746-9

Reference yield:

: dilithio (cyclo-octatetraenide)

: 85363-50-4
(2Z,4Z,6Z)-9-Benzyl-9-methyl-9-phosphonia-bicyclo[6.1.0]nona-2,4,6-triene

Guidance literature:: Multi-step reaction with 2 steps

1: 55 percent / diethyl ether / -78 °C

In diethyl ether;
DOI:10.1016/S0040-4039(00)85746-9