2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile

Base Information

Chemical Name:2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile
CAS No.:102284-01-5
Molecular Formula:3C₈Cl₂N₂O₂*4C₃₀H₁₈S₂
Molecular Weight:2451.44
Hs Code.:

Synonyms:2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile

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Chemical Property of 2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile

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Technology Process of 2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile

There total 2 articles about 2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 102283-97-6
2,11-diphenyl-3,10-dithiaperylene

: 84-58-2
2,3-dicyano-5,6-dichloro-p-benzoquinone

: 102284-01-5
2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile

Guidance literature:: In 1,1,2-trichloroethane; acetonitrile; for 2h;
DOI:10.1021/ja00272a048

Reference yield:

: 102283-95-4
2,11-diphenyl-1,2,11,12-tetrahydro-3,10-dithiaperylene

: 102284-01-5
2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 36 percent / N-chlorosuccinimide / CH₂Cl₂ / 1 h / -7 - 0 °C

2: 80 percent / acetonitrile; 1,1,2-trichloro-ethane / 2 h

With N-chloro-succinimide; In dichloromethane; 1,1,2-trichloroethane; acetonitrile;
DOI:10.1021/ja00272a048