2,11-diphenyl-3,10-dithiaperylene

Base Information

• Chemical Name: 2,11-diphenyl-3,10-dithiaperylene
• CAS No.: 102283-97-6
• Molecular Formula: C₃₀H₁₈S₂
• Molecular Weight: 442.605

Synonyms:2,11-diphenyl-3,10-dithiaperylene

Chemical Property of 2,11-diphenyl-3,10-dithiaperylene

Chemical Property:

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Technology Process of 2,11-diphenyl-3,10-dithiaperylene

There total 1 articles about 2,11-diphenyl-3,10-dithiaperylene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

2,11-diphenyl-1,2,11,12-tetrahydro-3,10-dithiaperylene (102283-95-4) → 2,11-diphenyl-3,10-dithiaperylene (102283-97-6)

Guidance literature:

With N-chloro-succinimide; In dichloromethane; at -7 - 0 ℃; for 1h;

DOI:10.1021/ja00272a048

Reference yield: 80.0%

2,11-diphenyl-3,10-dithiaperylene (102283-97-6) + 2,3-dicyano-5,6-dichloro-p-benzoquinone (84-58-2) → 2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile (102284-01-5)

Guidance literature:

In 1,1,2-trichloroethane; acetonitrile; for 2h;

DOI:10.1021/ja00272a048

Reference yield:

2,11-diphenyl-3,10-dithiaperylene (102283-97-6) → 5C30H18S2*9I(1-)

Guidance literature:

With tetrabutylammonium triiodide; In dichloromethane; by electrochemical method;

DOI:10.1021/ja00272a048

upstream raw materials:

2,11-diphenyl-1,2,11,12-tetrahydro-3,10-dithiaperylene

Downstream raw materials:

2,11-Diphenyl-3,10-dithia-perylene; compound with 4,5-dichloro-3,6-dioxo-cyclohexa-1,4-diene-1,2-dicarbonitrile

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