C₃₃H₄₀F₂N₆O₅S

Base Information

Chemical Name:C₃₃H₄₀F₂N₆O₅S
CAS No.:1620011-43-9
Molecular Formula:C₃₃H₄₀F₂N₆O₅S
Molecular Weight:670.781
Hs Code.:

C<sub>33</sub>H<sub>40</sub>F<sub>2</sub>N<sub>6</sub>O<sub>5</sub>S

Synonyms:C₃₃H₄₀F₂N₆O₅S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₄₀F₂N₆O₅S

Chemical Property:

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Technology Process of C₃₃H₄₀F₂N₆O₅S

There total 10 articles about C₃₃H₄₀F₂N₆O₅S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1270034-25-7
5-[(tert-butoxycarbonyl)amino]-2-(2,6-difluorophenyl)-1,3-thiazole-4-carboxylic acid

: 1620011-40-6
tert-butyl [(3S)-1-(3-amino-6,7-dihydro-5H-cyclopenta[b]pyridin-4-yl)piperidin-3-yl]carbamate

: 1620011-43-9
C₃₃H₄₀F₂N₆O₅S

Guidance literature:: With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; In N,N-dimethyl-formamide; at 20 - 30 ℃; for 16h;

Reference yield:

: 533-37-9
2,3-cyclopentenopyridine

: 1620011-43-9
C₃₃H₄₀F₂N₆O₅S

Guidance literature:: Multi-step reaction with 9 steps

1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 - 30 °C

2: trichlorophosphate / 3 h / 120 °C

3: sodium methylate / 18 h / 110 °C / Sealed tube

4: sulfuric acid; potassium nitrate / 4 h / 0 - 80 °C

5: hydrogen bromide; acetic acid / water / 0.67 h / 130 °C / Sealed tube

6: trichlorophosphate / 2 h / 110 °C / Sealed tube; Inert atmosphere

7: triethylamine / isopropyl alcohol / 0.5 h / 100 °C

8: iron; ammonium chloride / ethanol; water / 1 h / 80 °C / Sealed tube

9: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 - 30 °C

With sulfuric acid; hydrogen bromide; sodium methylate; iron; ammonium chloride; acetic acid; potassium nitrate; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; trichlorophosphate; In ethanol; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 90685-58-8
6,7-dihydro-5H-cyclopenta[b]pyridine 1-oxide

: 1620011-43-9
C₃₃H₄₀F₂N₆O₅S

Guidance literature:: Multi-step reaction with 8 steps

1: trichlorophosphate / 3 h / 120 °C

2: sodium methylate / 18 h / 110 °C / Sealed tube

3: sulfuric acid; potassium nitrate / 4 h / 0 - 80 °C

4: hydrogen bromide; acetic acid / water / 0.67 h / 130 °C / Sealed tube

5: trichlorophosphate / 2 h / 110 °C / Sealed tube; Inert atmosphere

6: triethylamine / isopropyl alcohol / 0.5 h / 100 °C

7: iron; ammonium chloride / ethanol; water / 1 h / 80 °C / Sealed tube

8: N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 16 h / 20 - 30 °C

With sulfuric acid; hydrogen bromide; sodium methylate; iron; ammonium chloride; acetic acid; potassium nitrate; triethylamine; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; trichlorophosphate; In ethanol; water; N,N-dimethyl-formamide; isopropyl alcohol;