methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate

Base Information

Chemical Name:methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate
CAS No.:99880-11-2
Molecular Formula:C₁₉H₁₉Cl₂NO₅
Molecular Weight:412.27
Hs Code.:

Synonyms:methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate

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Technology Process of methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate

There total 3 articles about methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 103772-83-4
4-(2,3-Dichloro-phenyl)-2,6-dimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-methyl ester 5-(2-methyl-[1,3]dioxolan-2-ylmethyl) ester

: 99880-11-2
methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate

Guidance literature:: With methanesulfonic acid; water; In ethanol; for 6h; Heating;
DOI:10.1248/cpb.34.1589

Reference yield:

: 86780-81-6
3-amino-2-crotonic acid 2,2-ethylenedioxy propyl ester

: 99880-11-2
methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: 27 percent / ethanol / 8 h / Heating

2: 89 percent / MeSO₃H, H₂O / ethanol / 6 h / Heating

With methanesulfonic acid; water; In ethanol;
DOI:10.1248/cpb.34.1589

Reference yield:

: 86780-80-5
2,2-ethylenedioxypropyl acetoacetate

: 99880-11-2
methyl 2-oxopropyl 4-(2,3-dichlorophenyl)-1,4-dihydro-2,6-dimethyl-3,5-pyridinedicarboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / NH₃ / methanol / 2.5 h / 0 - 5 °C

2: 27 percent / ethanol / 8 h / Heating

3: 89 percent / MeSO₃H, H₂O / ethanol / 6 h / Heating

With methanesulfonic acid; ammonia; water; In methanol; ethanol;
DOI:10.1248/cpb.34.1589