C₂₅H₃₁NO₃Si

Base Information

Chemical Name:C₂₅H₃₁NO₃Si
CAS No.:1603898-78-7
Molecular Formula:C₂₅H₃₁NO₃Si
Molecular Weight:421.612
Hs Code.:

C<sub>25</sub>H<sub>31</sub>NO<sub>3</sub>Si

Synonyms:C₂₅H₃₁NO₃Si

Suppliers and Price of C₂₅H₃₁NO₃Si

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₂₅H₃₁NO₃Si

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₂₅H₃₁NO₃Si

There total 5 articles about C₂₅H₃₁NO₃Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1603898-65-2
N,N-diethyl-O-([1-(3-methoxyphenyl)-3-(trimethylsilyl)]naphth-2-yl)-carbamate

: 1603898-78-7
C₂₅H₃₁NO₃Si

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; for 18h; Microwave irradiation;
DOI:10.1021/ol500707w

Reference yield:

: 135-19-3
β-naphthol

: 1603898-78-7
C₂₅H₃₁NO₃Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 1 h / 0 °C

2.1: 2,2,6,6-tetramethylpiperidinyl-lithium / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

2.2: 0.5 h / 0 - 20 °C / Inert atmosphere

3.1: Iodine monochloride / dichloromethane / 16 h / 20 °C

4.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / 16 h / Inert atmosphere; Reflux

5.1: lithium diisopropyl amide / tetrahydrofuran / 18 h / Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-tetramethylpiperidinyl-lithium; Iodine monochloride; sodium hydride; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; 4.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol500707w

Reference yield:

: 61912-14-9
2-naphthyl diethylcarbamate

: 1603898-78-7
C₂₅H₃₁NO₃Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,2,6,6-tetramethylpiperidinyl-lithium / tetrahydrofuran / 1.5 h / 0 °C / Inert atmosphere

1.2: 0.5 h / 0 - 20 °C / Inert atmosphere

2.1: Iodine monochloride / dichloromethane / 16 h / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / 1,2-dimethoxyethane / 16 h / Inert atmosphere; Reflux

4.1: lithium diisopropyl amide / tetrahydrofuran / 18 h / Microwave irradiation

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; 2,2,6,6-tetramethylpiperidinyl-lithium; Iodine monochloride; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; 3.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/ol500707w