N,N'-(ethane-1,2-diyl)bis

Base Information

Chemical Name:N,N'-(ethane-1,2-diyl)bis
CAS No.:125425-94-7
Molecular Formula:C₂₀H₂₂N₄O₄S₂
Molecular Weight:446.551
Hs Code.:

N,N'-(ethane-1,2-diyl)bis<N-(cyanomethyl)-4-methylbenzenesulfonamide>

Synonyms:N,N'-(ethane-1,2-diyl)bis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N'-(ethane-1,2-diyl)bis

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Technology Process of N,N'-(ethane-1,2-diyl)bis

There total 1 articles about N,N'-(ethane-1,2-diyl)bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 4403-78-5
ditosylethylenediamine

: 107-14-2
chloroacetonitrile

: 125425-94-7
N,N'-(ethane-1,2-diyl)bis

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; Ambient temperature;
DOI:10.1016/S0040-4039(00)99339-0

Reference yield: 97.0%

: 125425-94-7
N,N'-(ethane-1,2-diyl)bis

: 118852-30-5
N,N'-(ethane-1,2-diyl)bis

Guidance literature:: With diborane; In tetrahydrofuran; for 12h; Heating;
DOI:10.1016/S0040-4039(00)99339-0 DOI:10.1002/hlca.19960790302

Reference yield:

: 125425-94-7
N,N'-(ethane-1,2-diyl)bis

: 118852-31-6
4,7,13,16-tetratosyl-1,4,7,10,13,16-hexaazacyclooctadecane-2,9-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / diborane / tetrahydrofuran / 12 h / Heating

2: 38 percent / Et₃N / CH₂Cl₂; toluene / 7 h

With triethylamine; diborane; In tetrahydrofuran; dichloromethane; toluene;
DOI:10.1002/hlca.19960790302