6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine

Base Information

Chemical Name:6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine
CAS No.:1619938-53-2
Molecular Formula:C₄₅H₅₆N₆
Molecular Weight:680.98
Hs Code.:

Synonyms:6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine

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Chemical Property of 6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine

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Technology Process of 6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine

There total 5 articles about 6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1619938-54-3
2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine

: 1619938-55-4
(E)-4-((4-butylphenyl)diazenyl)naphthalen-1-aminium chloride

: 1619938-53-2
6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine

Guidance literature:: (E)-4-((4-butylphenyl)diazenyl)naphthalen-1-aminium chloride; With hydrogenchloride; acetic acid; sodium nitrite; In water; at 2 - 5 ℃;

2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine; With aminosulfonic acid; In ethanol; water; acetone; Cooling with ice;

Reference yield:

: 552-46-5
1-naphthylamine hydrochloride

: 1619938-53-2
6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium nitrite; hydrogenchloride / isopropyl alcohol; water / 1 h / 0 - 5 °C

2.1: sodium nitrite; acetic acid; hydrogenchloride / water / 2 - 5 °C

2.2: Cooling with ice

With hydrogenchloride; acetic acid; sodium nitrite; In water; isopropyl alcohol;

Reference yield:

: 479-27-6
naphthalene-1,8-diamine

: 1619938-53-2
6-((E)-(4-((E)-(4-butylphenyl)diazenyl)naphthalen-1-yl)diazenyl)-2-methyl-2-tridecyl-2,3-dihydro-1H-perimidine

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / isopropyl alcohol / 50 °C / Reflux

2.1: sodium nitrite; acetic acid; hydrogenchloride / water / 2 - 5 °C

2.2: Cooling with ice

With hydrogenchloride; acetic acid; sodium nitrite; In water; isopropyl alcohol;