dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate

Base Information

Chemical Name:dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate
CAS No.:429696-83-3
Molecular Formula:C₄₇H₆₀O₇
Molecular Weight:736.989
Hs Code.:

Synonyms:dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate

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Chemical Property of dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate

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Technology Process of dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate

There total 5 articles about dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 13036-02-7
Dimethyl 5-hydroxyisophthalate

: 213680-85-4
1,3-bis{[3,5-bis(tert-butyl)benzyl]oxy}-5-(bromomethyl)benzene

: 429696-83-3
dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate

Guidance literature:: With 18-crown-6 ether; tetra-(n-butyl)ammonium iodide; potassium carbonate; In acetone; Heating;
DOI:10.1016/S0040-4020(01)01113-9

Reference yield:

: 62938-08-3
3,5-di-tert-butylbenzyl bromide

: 429696-83-3
dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate

Guidance literature:: Multi-step reaction with 4 steps

1: 87 percent / K₂CO₃; 18-crown-6 / acetone / 24 h / Heating

2: 92 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

3: 84 percent / PBr₃ / diethyl ether / 2 h

4: 98 percent / K₂CO₃; 18-crown-6; tetrabutylammonium iodide / acetone / Heating

With lithium aluminium tetrahydride; 18-crown-6 ether; phosphorus tribromide; tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1016/S0040-4020(01)01113-9

Reference yield:

: 15181-11-0
3, 5-di-tert-butyltoluene

: 429696-83-3
dimethyl 5-(3,5-bis(3,5-di(tert-butyl)phenylmethoxy)phenylmethoxy)isophthalate

Guidance literature:: Multi-step reaction with 5 steps

1: 85 percent / NBS / Irradiation

2: 87 percent / K₂CO₃; 18-crown-6 / acetone / 24 h / Heating

3: 92 percent / LiAlH₄ / tetrahydrofuran / 0 - 20 °C

4: 84 percent / PBr₃ / diethyl ether / 2 h

5: 98 percent / K₂CO₃; 18-crown-6; tetrabutylammonium iodide / acetone / Heating

With N-Bromosuccinimide; lithium aluminium tetrahydride; 18-crown-6 ether; phosphorus tribromide; tetra-(n-butyl)ammonium iodide; potassium carbonate; In tetrahydrofuran; diethyl ether; acetone;
DOI:10.1016/S0040-4020(01)01113-9