5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine

Base Information

Chemical Name:5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine
CAS No.:162757-20-2
Molecular Formula:C₂₄H₂₁N₇O₆S
Molecular Weight:535.54
Hs Code.:

5'-amino-5'-deoxy-N<sup>6</sup>-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine

Synonyms:5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine

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Chemical Property of 5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine

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Technology Process of 5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine

There total 10 articles about 5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21950-36-7
5'-amino-5'-deoxy-2',3'-O-isopropylideneadenosine

: 162757-20-2
5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine

Guidance literature:: Multi-step reaction with 4 steps

1: 93 percent / pyridine / 4 h / 80 °C

2: 97 percent / pyridine / 2 h / Ambient temperature

3: 71 percent / CF₃CO₃₂H / H₂O / 0.67 h / Ambient temperature

4: t-BuOK / dimethylformamide / 3 h / 80 °C

With pyridine; C₂⁽²⁾HF₃O₃; potassium tert-butylate; In pyridine; water; N,N-dimethyl-formamide;
DOI:10.1080/15257779508014657

Reference yield:

: 162757-19-9
1-(N⁶-benzoyl-5'-deoxy-adenosin-5'-yl)-2-methyl-3-phenylsulfonyl-isothiourea

: 162757-20-2
5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine

Guidance literature:: With potassium tert-butylate; In N,N-dimethyl-formamide; at 80 ℃; for 3h;
DOI:10.1080/15257779508014657

Reference yield:

: 68144-26-3
5'-azido-5'-deoxy-N⁶-benzoyl-2',3'-O-isopropylidene adenosine

: 162757-20-2
5'-amino-5'-deoxy-N⁶-benzoyl-3'-O,5'-N-(N-phenylsulfonyliminocarbonyl)adenosine

Guidance literature:: Multi-step reaction with 6 steps

1: 66 percent / NH₃, MeOH / 40 h / Ambient temperature

2: 70 percent / H₂ / Pd-C / ethanol / 5 h / 2327.2 Torr

3: 93 percent / pyridine / 4 h / 80 °C

4: 97 percent / pyridine / 2 h / Ambient temperature

5: 71 percent / CF₃CO₃₂H / H₂O / 0.67 h / Ambient temperature

6: t-BuOK / dimethylformamide / 3 h / 80 °C

With pyridine; methanol; C₂⁽²⁾HF₃O₃; potassium tert-butylate; ammonia; hydrogen; palladium on activated charcoal; In pyridine; ethanol; water; N,N-dimethyl-formamide;
DOI:10.1080/15257779508014657