4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester)

Base Information

Chemical Name:4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester)
CAS No.:156235-28-8
Molecular Formula:C₂₆H₂₄N₂O₈
Molecular Weight:492.485
Hs Code.:

Synonyms:4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester)

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Chemical Property of 4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester)

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Technology Process of 4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester)

There total 7 articles about 4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 38256-25-6
dimethyl (E)-2-oxoglutaconate

: 156235-27-7
7-Amino-4-(benzyloxy)-5-methoxy-1H-indol-2-carbonsaeure-ethylester

: 156235-28-8
4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester)

Guidance literature:: With hydrogenchloride; copper diacetate; air; Yield given. Multistep reaction; 1.) CH₂Cl₂, 20 h, r.t.; 2.) CH₂Cl₂, 2 min; 3.) CH₂Cl₂, 24 h;
DOI:10.1002/hlca.19940770114

Reference yield:

: 2011-06-5
2-benzyloxy-3-methoxybenzaldehyde

: 156235-28-8
4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester)

Guidance literature:: Multi-step reaction with 5 steps

1: 60 percent / Na / ethanol / 1 h / 10 °C

2: 55 percent / xylene / 0.75 h / Heating

3: 38 percent / 100percent HNO₃ / acetic acid / 2 h / Ambient temperature

4: 54 percent / H₂ / 5percent Pt/C / tetrahydrofuran / 3 h

5: 2.) Cu(OAc)2*H₂O, gaseous HCl; 3.) air / 1.) CH₂Cl₂, 20 h, r.t.; 2.) CH₂Cl₂, 2 min; 3.) CH₂Cl₂, 24 h

With hydrogenchloride; copper diacetate; air; hydrogen; nitric acid; sodium; platinum on activated charcoal; In tetrahydrofuran; ethanol; acetic acid; xylene;
DOI:10.1002/hlca.19940770114

Reference yield:

: 100-39-0
benzyl bromide

: 156235-28-8
4-(Benzyloxy)-5-methoxy-1H-pyrrolo<3,2-h>chinolin-2,6,8-tricarbonsaeure-(2-ethyl-6,8-dimethylester)

Guidance literature:: Multi-step reaction with 6 steps

1: 96 percent / K₂CO₃, KI / dimethylformamide / 2 h / 70 °C

2: 60 percent / Na / ethanol / 1 h / 10 °C

3: 55 percent / xylene / 0.75 h / Heating

4: 38 percent / 100percent HNO₃ / acetic acid / 2 h / Ambient temperature

5: 54 percent / H₂ / 5percent Pt/C / tetrahydrofuran / 3 h

6: 2.) Cu(OAc)2*H₂O, gaseous HCl; 3.) air / 1.) CH₂Cl₂, 20 h, r.t.; 2.) CH₂Cl₂, 2 min; 3.) CH₂Cl₂, 24 h

With hydrogenchloride; copper diacetate; air; hydrogen; nitric acid; sodium; potassium carbonate; potassium iodide; platinum on activated charcoal; In tetrahydrofuran; ethanol; acetic acid; N,N-dimethyl-formamide; xylene;
DOI:10.1002/hlca.19940770114