N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide

Base Information

• Chemical Name: N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide
• CAS No.: 1200509-26-7
• Molecular Formula: C₂₃H₃₂N₂O₅S
• Molecular Weight: 448.583

Synonyms:N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide

Chemical Property of N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide

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Technology Process of N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide

There total 1 articles about N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

(1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetic acid (1200509-09-6) + toluene-4-sulfonamide (70-55-3) → N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide (1200509-26-7)

Guidance literature:

(1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere;

toluene-4-sulfonamide; In dichloromethane; at 20 ℃; for 96h; Inert atmosphere;

DOI:10.3762/bjoc.5.81

Reference yield: 42.0%

N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide (1200509-26-7) → N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide hydrochloride (1200509-17-6)

Guidance literature:

With hydrogenchloride; In water; at 20 ℃; for 20h; Inert atmosphere;

DOI:10.3762/bjoc.5.81

upstream raw materials:

(1S,2S,6R,7S,8S)-4-tert-butoxycarbonyl-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetic acid

toluene-4-sulfonamide

Downstream raw materials:

N-[(4-methylphenyl)sulfonyl] (1S,2S,6R,7S,8S)-4-azatricyclo[5.2.1.0(2,6)]decane-8-acetamide hydrochloride

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