2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol

Base Information

• Chemical Name: 2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol
• CAS No.: 1335029-87-2
• Molecular Formula: C₃₆H₃₆O₆S₂
• Molecular Weight: 628.81

Synonyms:2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol

Chemical Property of 2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol

Chemical Property:

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Technology Process of 2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol

There total 1 articles about 2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C35H33O6S2(1-)*Na(1+) + methyl iodide (74-88-4) → 2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol (1335029-87-2)

Guidance literature:

In tetrahydrofuran; mineral oil; at 20 ℃; for 16h;

DOI:10.1002/ejoc.200901156

Reference yield: 91.0%

2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol (1335029-87-2) → rac-1-O-benzoyl-2,4,6-tri-O-benzyl-3,5-dideoxy-myo-inositol

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 100 ℃; for 1h;

DOI:10.1002/ejoc.200901156

Reference yield: 72.0%

2,4,6-tri-O-benzyl-1,3-O-benzylidene-5-O-[(methylthio)thiocarbonyl]neo-inositol (1335029-87-2) → C29H32O6S2 (1335029-88-3) + S-methyl O-((1R,3r,5S,6R,7s,8S,9r)-6,8,9-tris(benzyloxy)-3-phenyl-2,4-dioxabicyclo[3.3.1]nonan-7-yl) carbonodithioate (1218932-89-8)

Guidance literature:

at 110 ℃; for 12h; Inert atmosphere;

DOI:10.1016/j.tet.2011.07.044

upstream raw materials:

methyl iodide

Downstream raw materials:

1,3-O-benzylidene-2,4,6-tri-o-benzyl-5-deoxy-myo-inositol

C₂₉H₃₂O₆S₂

S-methyl O-((1R,3r,5S,6R,7s,8S,9r)-6,8,9-tris(benzyloxy)-3-phenyl-2,4-dioxabicyclo[3.3.1]nonan-7-yl) carbonodithioate

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