(E)-diethyl 4,4'-(1-(5-chloro-1H-indol-2-yl)ethene-1,2-diyl)dibenzoate

Base Information

Chemical Name:(E)-diethyl 4,4'-(1-(5-chloro-1H-indol-2-yl)ethene-1,2-diyl)dibenzoate
CAS No.:1609205-87-9
Molecular Formula:C₂₈H₂₄ClNO₄
Molecular Weight:473.956
Hs Code.:

Synonyms:(E)-diethyl 4,4'-(1-(5-chloro-1H-indol-2-yl)ethene-1,2-diyl)dibenzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-diethyl 4,4'-(1-(5-chloro-1H-indol-2-yl)ethene-1,2-diyl)dibenzoate

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Technology Process of (E)-diethyl 4,4'-(1-(5-chloro-1H-indol-2-yl)ethene-1,2-diyl)dibenzoate

There total 2 articles about (E)-diethyl 4,4'-(1-(5-chloro-1H-indol-2-yl)ethene-1,2-diyl)dibenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 83536-13-4
bis(4-ethoxycarbonylphenyl)acetylene

: 1571899-52-9
5-chloro-N-(p-tolyl)-1H-indole-1-carboxamide

: 1609205-87-9
(E)-diethyl 4,4'-(1-(5-chloro-1H-indol-2-yl)ethene-1,2-diyl)dibenzoate

Guidance literature:: With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; In acetonitrile; at 100 ℃; for 20h; stereoselective reaction; Sealed tube;
DOI:10.1016/j.tetlet.2014.04.001

Reference yield:

: 17422-32-1
5-chloro-1H-indole

: 1609205-87-9
(E)-diethyl 4,4'-(1-(5-chloro-1H-indol-2-yl)ethene-1,2-diyl)dibenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate / acetonitrile / 20 h / 100 °C / Sealed tube

With dichloro(pentamethylcyclopentadienyl)rhodium (III) dimer; copper(II) acetate monohydrate; sodium hydride; In N,N-dimethyl-formamide; acetonitrile; mineral oil;
DOI:10.1016/j.tetlet.2014.04.001