4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine

Base Information

Chemical Name:4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine
CAS No.:132644-84-9
Molecular Formula:C₁₇H₂₁NO₅S
Molecular Weight:351.423
Hs Code.:

Synonyms:4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine

Chemical Property:

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Technology Process of 4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine

There total 3 articles about 4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 132644-75-8
2,2-dimethyl-5-(phenylsulfonyl)-4-piperidone

: 75-36-5
acetyl chloride

: 132644-84-9
4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine

Guidance literature:: With triethylamine; In dichloromethane; at 25 ℃; for 2h;
DOI:10.1021/jo00006a036

Reference yield:

: 85540-20-1
2,3-bis(phenylsulfonyl)-1,3-butadiene

: 132644-84-9
4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / CH₂Cl₂ / 24 h / 25 °C

2: 99 percent / Raney Nickel, CH₃OH / 0.33 h / Heating

3: 72 percent / Et₃N / CH₂Cl₂ / 2 h / 25 °C

With methanol; nickel; triethylamine; In dichloromethane;
DOI:10.1021/jo00006a036

Reference yield:

: 122603-49-0
2,2-dimethyl-4,5-endo-bis(phenylsulfonyl)-7-oxa-1-azabicyclo<2.2.1>heptane

: 132644-84-9
4-acetoxy-1-acetyl-6,6-dimethyl-3-(phenylsulfonyl)-1,2,5,6-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / Raney Nickel, CH₃OH / 0.33 h / Heating

2: 72 percent / Et₃N / CH₂Cl₂ / 2 h / 25 °C

With methanol; nickel; triethylamine; In dichloromethane;
DOI:10.1021/jo00006a036