C₁₂H₁₃BrN₂O₂

Base Information

Chemical Name:C₁₂H₁₃BrN₂O₂
CAS No.:1280538-41-1
Molecular Formula:C₁₂H₁₃BrN₂O₂
Molecular Weight:297.151
Hs Code.:

C<sub>12</sub>H<sub>13</sub>BrN<sub>2</sub>O<sub>2</sub>

Synonyms:C₁₂H₁₃BrN₂O₂

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Chemical Property of C₁₂H₁₃BrN₂O₂

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Technology Process of C₁₂H₁₃BrN₂O₂

There total 1 articles about C₁₂H₁₃BrN₂O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-bromo-6-nitrotoluene: 55289-35-5
2-bromo-6-nitrotoluene

: 5564-73-8
1-(dimethoxymethyl)pyrrolidine

: 1280538-41-1
C₁₂H₁₃BrN₂O₂

Guidance literature:: In N,N-dimethyl-formamide; for 16h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2011.08.094

Reference yield:

: 1280538-41-1
C₁₂H₁₃BrN₂O₂

: 52488-36-5
4-bromo-1H-indole

Guidance literature:: With iron; acetic acid; In ethanol; at 50 ℃; for 0.5h; Reflux; Inert atmosphere;
DOI:10.1016/j.tet.2011.08.094

Reference yield:

: 1280538-41-1
C₁₂H₁₃BrN₂O₂

: ethyl (E/Z)-3-[4-bromo-1-(4-toluenesulfonyl)indole-3-yl]-2-nitroacrylate

Guidance literature:: Multi-step reaction with 4 steps

1.1: iron; acetic acid / ethanol / 0.5 h / 50 °C / Reflux; Inert atmosphere

2.1: pyridine; trichlorophosphate / 0.75 h / 35 °C / Inert atmosphere; Cooling with ice

2.2: 0.03 h / 100 °C / Inert atmosphere; Cooling with ice

3.1: dmap; triethylamine / dichloromethane / 16 h / 20 °C / Inert atmosphere

4.1: titanium tetrachloride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

4.2: 0 °C / Inert atmosphere

With pyridine; dmap; titanium tetrachloride; iron; acetic acid; triethylamine; trichlorophosphate; In tetrahydrofuran; ethanol; dichloromethane; 2.1: Vilsmeier formylation / 4.1: Henry reaction;
DOI:10.1016/j.tet.2011.08.094