Technology Process of C27H29F2N3O4S
There total 1 articles about C27H29F2N3O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H29F2N3O4S;
With
sodium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
zinc(II) chloride;
In
tetrahydrofuran; 1,4-dioxane;
at 20 ℃;
for 0.5h;
Inert atmosphere;
(4-bromo-2-fluorophenyl)(cyclopropyl)methanone;
(2’,4’,6’-triisopropyl-[1,1’-biphenyl]-2-yl)-diphenylphosphine; palladium diacetate;
In
tetrahydrofuran; 1,4-dioxane;
at 100 ℃;
for 3h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hexamethyldisilazane / 1,4-dioxane; tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere
1.2: 0.5 h / 20 °C / Inert atmosphere
1.3: 3 h / 100 °C / Inert atmosphere
2.1: dipotassium hydrogenphosphate; sodium persulfate / acetonitrile; water / 0.75 h / 75 °C
2.2: pH ~ 10
With
dipotassium hydrogenphosphate; sodium persulfate; sodium hexamethyldisilazane;
In
tetrahydrofuran; 1,4-dioxane; water; acetonitrile;