4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid

Base Information

Chemical Name:4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid
CAS No.:1228560-66-4
Molecular Formula:C₁₈H₁₄ClN₃O₅S
Molecular Weight:419.845
Hs Code.:

Synonyms:4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid

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Chemical Property of 4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid

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Technology Process of 4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid

There total 3 articles about 4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1228560-65-3
4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarbaldehyde

: 1228560-66-4
4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid

Guidance literature:: With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; In water; acetone; at 20 ℃; for 16h;

Reference yield:

: 959137-49-6
5-(4-chlorophenyl)-4-cyclopropyl-2,4-dihydro-3H-1,2,4-triazol-3-one

: 1228560-66-4
4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; paraffin / 12 h / 0 - 20 °C

2: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogen phosphate monohydrate / water; acetone / 16 h / 20 °C

With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium hydride; In water; N,N-dimethyl-formamide; acetone; paraffin;

Reference yield:

: 85822-16-8
4-formylbenzene-1-sulfonyl chloride

: 1228560-66-4
4-{[3-(4-Chlorophenyl)-4-cyclopropyl-5-oxo-4,5-dihydro-1H-1,2,4-triazol-1-yl]sulphonyl}benzenecarboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydride / N,N-dimethyl-formamide; paraffin / 12 h / 0 - 20 °C

2: 2-methyl-but-2-ene; sodium chlorite; sodium dihydrogen phosphate monohydrate / water; acetone / 16 h / 20 °C

With sodium chlorite; sodium dihydrogen phosphate monohydrate; 2-methyl-but-2-ene; sodium hydride; In water; N,N-dimethyl-formamide; acetone; paraffin;