(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

Base Information

Chemical Name:(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol
CAS No.:1253890-67-3
Molecular Formula:C₂₁H₃₈O₃Si₂
Molecular Weight:394.702
Hs Code.:

Synonyms:(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

Suppliers and Price of (+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

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Technology Process of (+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

There total 1 articles about (+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 1253890-66-2
(+/-)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]-prop-2-en-1-yl acetate

: 1253890-67-3
(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

: 1253890-68-4
(-)-(S)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]-prop-2-en-1-yl acetate

Guidance literature:: With Pseudomonas cepacia lipase; water; In 1,4-dioxane; at 25 ℃; for 7h; pH=7; optical yield given as %ee; enantioselective reaction; aq. phosphate buffer; Enzymatic reaction;
DOI:10.1016/j.tet.2010.07.074

Reference yield: 56.0%

: 1253890-67-3
(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

: 26164-26-1
(S)-2-methoxy-2-phenylacetic acid

: 1253890-78-6
(+)-(R)-1-(3',4'-bis(tert-butyldimethylsilyloxy)phenyl)-allyl (S)-2-methoxy-2-phenylacetate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2010.07.074

Reference yield: 45.0%

: 1253890-67-3
(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

: 3966-32-3
(R)-methoxyphenylacetic acid

: 1253890-77-5
(-)-(R)-1-(3',4'-bis(tert-butyldimethylsilyloxy)phenyl)allyl (R)-2-methoxy-2-phenylacetate

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2010.07.074