(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-yl allyl ether

Base Information

Chemical Name:(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-yl allyl ether
CAS No.:1253890-70-8
Molecular Formula:C₂₄H₄₂O₃Si₂
Molecular Weight:434.767
Hs Code.:

Synonyms:(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-yl allyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-yl allyl ether

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Technology Process of (+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-yl allyl ether

There total 1 articles about (+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-yl allyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1253890-67-3
(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol

: 106-95-6
allyl bromide

: 1253890-70-8
(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-yl allyl ether

Guidance literature:: (+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-ol; With lithium hexamethyldisilazane; In tetrahydrofuran; at 0 ℃; Inert atmosphere;

allyl bromide; In tetrahydrofuran; at 0 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2010.07.074

Reference yield: 98.0%

: 1253890-70-8
(+)-(R)-1-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]prop-2-en-1-yl allyl ether

: 1253890-71-9
(+)-(R)-2-[(3',4'-bis-(tert-butyldimethylsilanoxy)phenyl)]-2,5-dihydrofuran

Guidance literature:: With Grubbs catalyst first generation; In dichloromethane; at 25 ℃; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2010.07.074