6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole

Base Information

• Chemical Name: 6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole
• CAS No.: 80750-63-6
• Molecular Formula: C₃₆H₂₈N₂O₂P₂
• Molecular Weight: 582.578

Synonyms:6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole

Chemical Property of 6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole

There total 7 articles about 6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

diphenylphosphonic acid o-aminophenyl ester (93638-67-6) → 6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole (80750-63-6)

Guidance literature:

With tetrachloromethane; triethylamine; triphenylphosphine; In tetrahydrofuran; Heating; other solvents, also with Ph₃P*Br₂;

DOI:10.1016/S0040-4039(00)98072-9

Reference yield: 71.0%

2,3-dihydro-2-methoxy-2,2-diphenyl-1,3,2-benzoxazaphosph(V)ole (67201-31-4) → 6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole (80750-63-6)

Guidance literature:

In toluene; at 110 ℃; for 1.5h;

Reference yield: 10.0%

2-amino-phenol (95-55-6) + Diphenylphosphinic chloride (1499-21-4) → diphenylphosphonic acid o-aminophenyl ester (93638-67-6) + 6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole (80750-63-6)

Guidance literature:

In tetrahydrofuran; 1,4-dioxane;

DOI:10.1016/S0040-4039(00)98072-9

upstream raw materials:

2,3-dihydro-2-methoxy-2,2-diphenyl-1,3,2-benzoxazaphosph(V)ole

diphenylphosphonic acid o-aminophenyl ester

2-ethoxy-2,3-dihydro-2,2-diphenyl-1,3,2-benzoxazaphosph(V)ole

2-neopentyloxy-2,3-dihydro-2,2-diphenyl-1,3,2-benzoxazaphosph(V)ole

Downstream raw materials:

2-(3,3-dimethyl-1,3-diazapropenyl)phenyl diphenylphosphinate

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 80750-63-6 6,6,13,13-tetrahydro-6,6,13,13-tetraphenyl<1,3,2,4>diazadiphospheto<2,1-b:4,3-b'>bis<1,3,2>benzoxazaphosph(V)ole

Send

Send

Metric Ton KG G Pound L ML

Send

Send