endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

Base Information

Chemical Name:endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline
CAS No.:86557-88-2
Molecular Formula:C₂₀H₂₂N₂O₂S
Molecular Weight:354.473
Hs Code.:

endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenz<f>isoindoline

Synonyms:endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

Suppliers and Price of endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

Chemical Property:

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Technology Process of endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

There total 3 articles about endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 86557-85-9
endo-3a,9a-dihydro-2-methyl-1,3-dioxo-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

: 86557-88-2
endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

Guidance literature:: With diborane; In tetrahydrofuran; 30 min at 0 deg C, then 4.5 h at room temp.;
DOI:10.1016/S0040-4020(01)91911-8

Reference yield:

: 930-88-1
N-methylmaleimide

: 86557-88-2
endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 25 h / Heating

2: 60 percent / diborane / tetrahydrofuran / 30 min at 0 deg C, then 4.5 h at room temp.

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; diborane; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(01)91911-8

Reference yield:

: 32372-83-1
2(toluene-p-sulphonyl)isoindoline

: 86557-88-2
endo-3a,9a-dihydro-2-methyl-4,9-(toluene-p-sulphonyl)epiminobenzisoindoline

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 2,3-dichloro-5,6-dicyanobenzoquinone / benzene / 25 h / Heating

2: 60 percent / diborane / tetrahydrofuran / 30 min at 0 deg C, then 4.5 h at room temp.

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; diborane; In tetrahydrofuran; benzene;
DOI:10.1016/S0040-4020(01)91911-8