ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate

Base Information

Chemical Name:ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate
CAS No.:27331-97-1
Molecular Formula:C₁₂H₁₃NO₅
Molecular Weight:251.239
Hs Code.:

Synonyms:ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate

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Technology Process of ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate

There total 2 articles about ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 2881-83-6
ethyl 4-methoxybenzoylacetate

: 27331-97-1
ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate

Guidance literature:: With acetic acid; sodium nitrite; for 2h;
DOI:10.1248/cpb.41.1521

Reference yield:

: 94-30-4
ethyl 4-methoxybenzoate

: 27331-97-1
ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium / Reinigung ueber das Kupfersalz

2: glacial acetic acid; sodium nitrite

With sodium; acetic acid; sodium nitrite;

Reference yield: 85.0%

: 27331-97-1
ethyl α-hydroxyimino-β-oxo-4-methoxybenzenepropionate

: erythro-β-(4-methoxyphenyl)serine ethyl ester hydrochloride

Guidance literature:: With hydrogenchloride; hydrogen; palladium on activated charcoal; In ethanol; under 760 Torr; Ambient temperature;
DOI:10.1248/cpb.41.1521