1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane

Base Information

Chemical Name:1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane
CAS No.:852948-98-2
Molecular Formula:C₂₁H₂₇BrO₂
Molecular Weight:391.348
Hs Code.:

Synonyms:1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane

Chemical Property:

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Technology Process of 1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane

There total 6 articles about 1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 852948-97-1
3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propanol

: 852948-98-2
1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In diethyl ether; at 20 ℃; for 16h;

Reference yield:

: 322472-55-9
3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)benzaldehyde

: 852948-98-2
1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 1 h / 20 °C

2.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

4.1: carbon tetrabromide; triphenylphosphine / diethyl ether / 16 h / 20 °C

With carbon tetrabromide; hydrogen; sodium hydride; diisobutylaluminium hydride; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; diethyl ether;

Reference yield:

: 852948-96-0
trans-3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]-prop-2-en-1-ol

: 852948-98-2
1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

2: carbon tetrabromide; triphenylphosphine / diethyl ether / 16 h / 20 °C

With carbon tetrabromide; hydrogen; triphenylphosphine; palladium 10% on activated carbon; In methanol; diethyl ether;