diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate

Base Information

Chemical Name:diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate
CAS No.:852948-99-3
Molecular Formula:C₂₅H₃₇O₅P
Molecular Weight:448.54
Hs Code.:

Synonyms:diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate

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Chemical Property of diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate

Chemical Property:

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Technology Process of diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate

There total 6 articles about diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 852948-98-2
1-bromo-3-[3,5-dimethyl 4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propane

: 122-52-1
triethyl phosphite

: 852948-99-3
diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate

Guidance literature:: In N,N-dimethyl-formamide; for 2.5h; Heating / reflux;

Reference yield:

: 322472-55-9
3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)benzaldehyde

: 852948-99-3
diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hydride / tetrahydrofuran / 0.5 h / 0 - 20 °C

1.2: 1 h / 20 °C

2.1: diisobutylaluminium hydride / tetrahydrofuran / 2 h / 0 - 20 °C

3.1: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

4.1: carbon tetrabromide; triphenylphosphine / diethyl ether / 16 h / 20 °C

5.1: N,N-dimethyl-formamide / 2.5 h / Heating / reflux

With carbon tetrabromide; hydrogen; sodium hydride; diisobutylaluminium hydride; triphenylphosphine; palladium 10% on activated carbon; In tetrahydrofuran; methanol; diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 852948-96-0
trans-3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]-prop-2-en-1-ol

: 852948-99-3
diethyl 3-[3,5-dimethyl-4-(3'-iso-propyl-4'-methoxyphenoxy)phenyl]propylphosphonate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / methanol / 6 h / 20 °C

2: carbon tetrabromide; triphenylphosphine / diethyl ether / 16 h / 20 °C

3: N,N-dimethyl-formamide / 2.5 h / Heating / reflux

With carbon tetrabromide; hydrogen; triphenylphosphine; palladium 10% on activated carbon; In methanol; diethyl ether; N,N-dimethyl-formamide;