2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl

Base Information

Chemical Name:2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl
CAS No.:396725-73-8
Molecular Formula:C₃₁H₂₉NO₄S
Molecular Weight:511.642
Hs Code.:

Synonyms:2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl

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Chemical Property of 2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl

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Technology Process of 2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl

There total 6 articles about 2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4'-{[1-(3-tert-Butoxycarbonylsulfanyl-phenyl)-meth-(E)-ylidene]-amino}-[1,1';2',1'']terphenyl-3-carboxylic acid

: 396725-73-8
2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl

Guidance literature:: With sodium tetrahydroborate; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1021/jm0103099

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 396725-73-8
2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / DMAP; Et₃N / tetrahydrofuran / 20 °C

2: Et₃N / tetrahydrofuran / 0.5 h / 0 °C

3: NaBH₄ / tetrahydrofuran / 1 h / 0 °C

4: 60 percent / oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -70 - 20 °C

5: AcOH / CH₂Cl₂ / 1 h / 20 °C

6: 10 mg / NaBH₄ / CH₂Cl₂ / 2 h / 20 °C

With dmap; sodium tetrahydroborate; oxalyl dichloride; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 4: Swern oxidation;
DOI:10.1021/jm0103099

Reference yield:

: 4869-59-4
3-mercapto benzoic acid

: 396725-73-8
2-phenyl-4-[3-S-(t-butoxycarbonyl)mercaptobenzyl]amino-3'-carboxybiphenyl

Guidance literature:: Multi-step reaction with 6 steps

1: 97 percent / DMAP; Et₃N / tetrahydrofuran / 20 °C

2: Et₃N / tetrahydrofuran / 0.5 h / 0 °C

3: NaBH₄ / tetrahydrofuran / 1 h / 0 °C

4: 60 percent / oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -70 - 20 °C

5: AcOH / CH₂Cl₂ / 1 h / 20 °C

6: 10 mg / NaBH₄ / CH₂Cl₂ / 2 h / 20 °C

With dmap; sodium tetrahydroborate; oxalyl dichloride; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 4: Swern oxidation;
DOI:10.1021/jm0103099