THIOCARBONIC ACID O-TERT-BUTYL ESTER S-(3-FORMYL-PHENYL) ESTER

Base Information

Chemical Name:THIOCARBONIC ACID O-TERT-BUTYL ESTER S-(3-FORMYL-PHENYL) ESTER
CAS No.:396725-72-7
Molecular Formula:C12H14 O3 S
Molecular Weight:238.3
Hs Code.:
Mol file:396725-72-7.mol

Synonyms:THIOCARBONIC ACID O-TERT-BUTYL ESTER S-(3-FORMYL-PHENYL) ESTER

Suppliers and Price of THIOCARBONIC ACID O-TERT-BUTYL ESTER S-(3-FORMYL-PHENYL) ESTER

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Labseeker
thiocarbonicacido-tert-butylesterS-(3-formyl-phenyl)ester 95
10g
$ 2933.00

Total 2 raw suppliers

Chemical Property of THIOCARBONIC ACID O-TERT-BUTYL ESTER S-(3-FORMYL-PHENYL) ESTER

Chemical Property:

Boiling Point:345.6±44.0 °C(Predicted)
PSA：68.67000
Density:1.17±0.1 g/cm3(Predicted)
LogP:3.52630

Purity/Quality:

95% ^*data from raw suppliers

thiocarbonicacido-tert-butylesterS-(3-formyl-phenyl)ester 95 ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of THIOCARBONIC ACID O-TERT-BUTYL ESTER S-(3-FORMYL-PHENYL) ESTER

There total 4 articles about THIOCARBONIC ACID O-TERT-BUTYL ESTER S-(3-FORMYL-PHENYL) ESTER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 396725-71-6
3-S-(t-butoxycarbonyl)mercaptobenzyl alcohol

: 396725-72-7
3-S-(t-butoxycarbonyl)mercaptobenzaldehyde

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -70 - 20 ℃;
DOI:10.1021/jm0103099

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 396725-72-7
3-S-(t-butoxycarbonyl)mercaptobenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / DMAP; Et₃N / tetrahydrofuran / 20 °C

2: Et₃N / tetrahydrofuran / 0.5 h / 0 °C

3: NaBH₄ / tetrahydrofuran / 1 h / 0 °C

4: 60 percent / oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -70 - 20 °C

With dmap; sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 4: Swern oxidation;
DOI:10.1021/jm0103099

Reference yield:

: 4869-59-4
3-mercapto benzoic acid

: 396725-72-7
3-S-(t-butoxycarbonyl)mercaptobenzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / DMAP; Et₃N / tetrahydrofuran / 20 °C

2: Et₃N / tetrahydrofuran / 0.5 h / 0 °C

3: NaBH₄ / tetrahydrofuran / 1 h / 0 °C

4: 60 percent / oxalyl chloride; DMSO; Et₃N / CH₂Cl₂ / -70 - 20 °C

With dmap; sodium tetrahydroborate; oxalyl dichloride; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 4: Swern oxidation;
DOI:10.1021/jm0103099