tri(ethoxy)(phenoxy)silane

Base Information

• Chemical Name: tri(ethoxy)(phenoxy)silane
• CAS No.: 18023-36-4
• Molecular Formula: C₁₂H₂₀O₄Si
• Molecular Weight: 256.374

Synonyms:tri(ethoxy)(phenoxy)silane

Chemical Property of tri(ethoxy)(phenoxy)silane

Chemical Property:

Purity/Quality:

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Technology Process of tri(ethoxy)(phenoxy)silane

There total 7 articles about tri(ethoxy)(phenoxy)silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

Triethoxysilane (998-30-1) + phenol (108-95-2,27073-41-2) → tri(ethoxy)(phenoxy)silane (18023-36-4)

Guidance literature:

With [MnN(salen-3,5-^tBu₂)]; In [D₃]acetonitrile; at 80 ℃; for 3h;

DOI:10.1039/c5cy01912e

Reference yield:

tetraethoxy orthosilicate (78-10-4) + phenol (108-95-2,27073-41-2) → tri(ethoxy)(phenoxy)silane (18023-36-4) + di(ethoxy)di(phenoxy)silane (1521-15-9)

Guidance literature:

With CBV₇₈₀; at 70 ℃; for 0.416667h; Overall yield = 64.0 %; Microwave irradiation;

Reference yield:

Triethoxysilane (998-30-1) + allyl phenyl ether (1746-13-0) → γ-phenoxypropyltriethoxysilane (58096-84-7) + tri(ethoxy)(phenoxy)silane (18023-36-4)

Guidance literature:

With C₁₄H₁₂*2C₁₈H₁₅P*Ni; at 125 ℃; for 25h; Inert atmosphere;

DOI:10.1134/S1070363210040079

upstream raw materials:

tetraethoxy orthosilicate

phenol

Triethoxysilane

tetraphenoxysilane

Downstream raw materials:

hexaethoxydisiloxane

di(ethoxy)di(phenoxy)silane

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