2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate

Base Information

• Chemical Name: 2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate
• CAS No.: 169049-82-5
• Molecular Formula: C₄₃H₃₁N₃O₁₁
• Molecular Weight: 765.733

Synonyms:2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate

Chemical Property of 2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate

Chemical Property:

Purity/Quality:

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Technology Process of 2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate

There total 1 articles about 2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2-(4-nitrophenyl)ethyl 5-amino-2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}benzoate (195875-06-0) + phenyl chloroformate (1885-14-9) → 2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate (169049-82-5)

Guidance literature:

With pyridine; dmap; at 20 ℃;

DOI:10.1002/hlca.201000253

Reference yield: 84.0%

N2-{{2-[2-(2-aminoethoxy)ethoxy]ethyl}amino}-2'-deoxy-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}guanosine (1263364-06-2) + 2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate (169049-82-5) → 2-(4-nitrophenyl)ethyl 5-{{{{2-{2-{2-{{9-(2'-deoxy-β-D-ribofuranosyl)-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}-6,9-dihydro-6-oxo-1H-purin-2-yl}amino}ethoxy}ethoxy}ethyl}amino}carbonyl}amino}-2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}benzoate (1263364-07-3)

Guidance literature:

With pyridine; dmap; In N,N-dimethyl-formamide; at 70 ℃; for 0.75h;

DOI:10.1002/hlca.201000253

Reference yield:

2-(4-nitrophenyl)ethyl 2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}-5-[(phenoxycarbonyl)amino]benzoate (169049-82-5) + C33H41N11O13 (169049-80-3) → C70H66N14O23 (1263364-12-0)

Guidance literature:

With pyridine; dmap; In N,N-dimethyl-formamide; at 60 ℃; for 4h;

DOI:10.1002/hlca.201000253

upstream raw materials:

2-(4-nitrophenyl)ethyl 5-amino-2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}benzoate

phenyl chloroformate

Downstream raw materials:

2-(4-nitrophenyl)ethyl 5-{{{{2-{2-{2-{{9-(2'-deoxy-β-D-ribofuranosyl)-1-{2-[(2,4-dinitrophenyl)methylamino]ethyl}-6,9-dihydro-6-oxo-1H-purin-2-yl}amino}ethoxy}ethoxy}ethyl}amino}carbonyl}amino}-2-{6-[2-(4-nitrophenyl)ethoxy]-3-oxo-3H-xanthen-9-yl}benzoate

C₇₀H₆₆N₁₄O₂₃

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