ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate

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Chemical Name:ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate
CAS No.:1187551-45-6
Molecular Formula:C₂₂H₁₇BrFNO₅
Molecular Weight:474.283
Hs Code.:

Synonyms:ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate

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Chemical Property of ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate

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Technology Process of ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate

There total 1 articles about ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 1187551-48-9
3-acetyl-6-bromo-1-((4-fluorophenyl)methyl)-4(1H)-quinolinone

: 95-92-1
oxalic acid diethyl ester

: 1187551-45-6
ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate

Guidance literature:: With hydrogenchloride; sodium ethanolate; In tetrahydrofuran; at 20 ℃; for 20h;
DOI:10.1016/j.bmcl.2009.06.044

Reference yield: 83.0%

: 1187551-45-6
ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate

: 1187551-46-7
[6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoic acid

Guidance literature:: ethyl [6-bromo-1-(4-fluorophenylmethyl)-4(1H)-quinolinon-3-yl]-4-hydroxy-2-oxo-3-butenoate; With sodium hydroxide; In tetrahydrofuran; methanol; water; for 1.15h;

With hydrogenchloride; water; In tetrahydrofuran; methanol; water; at 20 ℃;
DOI:10.1016/j.bmcl.2009.06.044