7-benzyloxy-4-oxo-2-octenal

Base Information

Chemical Name:7-benzyloxy-4-oxo-2-octenal
CAS No.:370863-15-3
Molecular Formula:C₁₅H₁₈O₃
Molecular Weight:246.306
Hs Code.:

Synonyms:7-benzyloxy-4-oxo-2-octenal

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Chemical Property of 7-benzyloxy-4-oxo-2-octenal

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Technology Process of 7-benzyloxy-4-oxo-2-octenal

There total 5 articles about 7-benzyloxy-4-oxo-2-octenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.9%

: 370863-14-2
7-benzyloxy-2-octene-1,4-diol

: 370863-15-3
7-benzyloxy-4-oxo-2-octenal

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 20 ℃; for 6h;

Reference yield:

: 52657-84-8
(±)-3-benzyloxybutan-1-ol

: 370863-15-3
7-benzyloxy-4-oxo-2-octenal

Guidance literature:: Multi-step reaction with 4 steps

1.1: 85 percent / Ph₃P; imidazole; I₂ / diethyl ether / 0 °C

2.1: t-BuLi / diethyl ether; pentane / 1 h / -78 °C

2.2: 50 percent / diethyl ether; pentane / -78 - 20 °C

3.1: 89 percent / stannous chloride / methanol / 6 h / 20 °C

4.1: 77.9 percent / iodoxybenzoic acid / dimethylsulfoxide / 6 h / 20 °C

With 1H-imidazole; iodine; tert.-butyl lithium; triphenylphosphine; tin(ll) chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; diethyl ether; dimethyl sulfoxide; pentane;

Reference yield:

: 90812-70-7
3-benzyloxy-1-iodobutane

: 370863-15-3
7-benzyloxy-4-oxo-2-octenal

Guidance literature:: Multi-step reaction with 3 steps

1.1: t-BuLi / diethyl ether; pentane / 1 h / -78 °C

1.2: 50 percent / diethyl ether; pentane / -78 - 20 °C

2.1: 89 percent / stannous chloride / methanol / 6 h / 20 °C

3.1: 77.9 percent / iodoxybenzoic acid / dimethylsulfoxide / 6 h / 20 °C

With tert.-butyl lithium; tin(ll) chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In methanol; diethyl ether; dimethyl sulfoxide; pentane;