1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde O-methyl oxime

Base Information

Chemical Name:1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde O-methyl oxime
CAS No.:1376614-91-3
Molecular Formula:C₂₃H₂₄ClN₇O
Molecular Weight:449.943
Hs Code.:

Synonyms:1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde O-methyl oxime

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde O-methyl oxime

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Technology Process of 1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde O-methyl oxime

There total 2 articles about 1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde O-methyl oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 593-56-6
N-methoxylamine hydrochloride

: 114798-36-6
EXP 3179

: 1376614-91-3
1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde O-methyl oxime

Guidance literature:: With potassium hydrogencarbonate; In ethanol; water; at 60 ℃; for 16h;

Reference yield:

: 124750-99-8
cozaar

: 1376614-91-3
1-((2'-(2H-tetrazol-5-yl)-[1,1'-biphenyl]-4-yl)methyl)-2-butyl-4-chloro-1H-imidazole-5-carbaldehyde O-methyl oxime

Guidance literature:: Multi-step reaction with 2 steps

1: methanesulfonic acid; manganese(IV) oxide / tert-butyl alcohol / 16 h / Reflux

2: potassium hydrogencarbonate / ethanol; water / 16 h / 60 °C

With manganese(IV) oxide; methanesulfonic acid; potassium hydrogencarbonate; In ethanol; water; tert-butyl alcohol;