N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine

Base Information

Chemical Name:N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine
CAS No.:219518-92-0
Molecular Formula:C₂₄H₂₁N₃O₃
Molecular Weight:399.449
Hs Code.:

N<sup>1</sup>-(3-cyanobenzoyl)-N<sup>2</sup>-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine

Synonyms:N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine

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Chemical Property of N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine

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Technology Process of N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine

There total 5 articles about N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 610-81-1
4-hydroxy-2-nitroaniline

: 219518-92-0
N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / imidazole / dimethylformamide / 5 h

2: 94 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

3: H₂ / 10percent Pd/C / tetrahydrofuran / 12 h

4: pyridine / CH₂Cl₂ / 0.17 h / 0 - 20 °C

5: 91 percent / TBAF / tetrahydrofuran / 1 h

With pyridine; 1H-imidazole; tetrabutyl ammonium fluoride; hydrogen; 10percent Pd/C; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1: Silylation / 2: Acylation / 3: Reduction / 4: Acylation / 5: Desilylation;
DOI:10.1021/jm9903287

Reference yield:

: 215656-99-8
4-{[tert-butyl(dimethyl)silyl]oxy}-2-nitroaniline

: 219518-92-0
N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine

Guidance literature:: Multi-step reaction with 4 steps

1: 94 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

2: H₂ / 10percent Pd/C / tetrahydrofuran / 12 h

3: pyridine / CH₂Cl₂ / 0.17 h / 0 - 20 °C

4: 91 percent / TBAF / tetrahydrofuran / 1 h

With pyridine; tetrabutyl ammonium fluoride; hydrogen; 10percent Pd/C; In tetrahydrofuran; dichloromethane; 1: Acylation / 2: Reduction / 3: Acylation / 4: Desilylation;
DOI:10.1021/jm9903287

Reference yield:

: 219518-89-5
N-(3-cyanobenzoyl)-2-nitro-4-(tert-butyldimethylsilyloxy)aniline

: 219518-92-0
N¹-(3-cyanobenzoyl)-N²-(4-isopropylbenzoyl)-4-hydroxy-1,2-benzenediamine

Guidance literature:: Multi-step reaction with 3 steps

1: H₂ / 10percent Pd/C / tetrahydrofuran / 12 h

2: pyridine / CH₂Cl₂ / 0.17 h / 0 - 20 °C

3: 91 percent / TBAF / tetrahydrofuran / 1 h

With pyridine; tetrabutyl ammonium fluoride; hydrogen; 10percent Pd/C; In tetrahydrofuran; dichloromethane; 1: Reduction / 2: Acylation / 3: Desilylation;
DOI:10.1021/jm9903287