N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide

Base Information

Chemical Name:N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide
CAS No.:899234-72-1
Molecular Formula:C₁₅H₁₆N₄O₄S₂
Molecular Weight:380.448
Hs Code.:

Synonyms:N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide

Chemical Property:

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Technology Process of N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide

There total 3 articles about N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 51908-29-3
4-isothiocyanatobenzene sulfonamide

: 3290-99-1
4-methoxybenzoic acid hydrazide

: 899234-72-1
N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide

Guidance literature:: In ethanol; Reflux;
DOI:10.1016/j.bmc.2014.01.055

Reference yield:

: 63-74-1
sulfanilamide

: 899234-72-1
N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 3 steps

1: methanol / 0.17 h / 0 °C

2: sodium hydrogencarbonate; iodine / ethyl acetate; water / Cooling with ice

3: ethanol / Reflux

With iodine; sodium hydrogencarbonate; In methanol; ethanol; water; ethyl acetate;
DOI:10.1016/j.bmc.2014.01.055

Reference yield:

: 57381-11-0
triethylamine thiocarbamate

: 899234-72-1
N-[4-(aminosulfonyl)phenyl]-2-(4-methoxybenzoyl)-1-hydrazinecarbothioamide

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate; iodine / ethyl acetate; water / Cooling with ice

2: ethanol / Reflux

With iodine; sodium hydrogencarbonate; In ethanol; water; ethyl acetate;
DOI:10.1016/j.bmc.2014.01.055