benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Base Information

Chemical Name:benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside
CAS No.:81086-77-3
Molecular Formula:C₂₅H₃₁NO₇
Molecular Weight:457.524
Hs Code.:

Synonyms:benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

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Technology Process of benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

There total 2 articles about benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 81086-76-2
benzyl 2-deoxy-5,6-O-isopropylidene-2-methylamino-β-D-glucofuranoside

: 81086-77-3
benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Guidance literature:: With sodium carbonate; In 1,4-dioxane; at 0 ℃; for 1.5h;
DOI:10.1016/S0008-6215(00)80680-1

Reference yield:

: 58886-40-1
benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

: 81086-77-3
benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / lithium aluminium hydride / tetrahydrofuran / 19 h / Heating

2: 88 percent / 0.5 M sodium carbonate / dioxane / 1.5 h / 0 °C

With lithium aluminium tetrahydride; sodium carbonate; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/S0008-6215(00)80680-1