benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Base Information

Chemical Name:benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside
CAS No.:81086-79-5
Molecular Formula:C₂₈H₃₅NO₉
Molecular Weight:529.587
Hs Code.:

Synonyms:benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Suppliers and Price of benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

There total 3 articles about benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 598-78-7,7474-05-7,29617-66-1,62138-52-7
L-2-chloropropionic acid

: 81086-77-3
benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

: 81086-79-5
benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Guidance literature:: With sodium hydride; In 1,4-dioxane; at 60 ℃; for 2.5h;
DOI:10.1016/S0008-6215(00)80680-1

Reference yield:

: 58886-40-1
benzyl 2-(benzyloxycarbonyl)amino-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

: 81086-79-5
benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / lithium aluminium hydride / tetrahydrofuran / 19 h / Heating

2: 88 percent / 0.5 M sodium carbonate / dioxane / 1.5 h / 0 °C

3: 60 percent / sodium hydride / dioxane / 2.5 h / 60 °C

With lithium aluminium tetrahydride; sodium hydride; sodium carbonate; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1016/S0008-6215(00)80680-1

Reference yield:

: 81086-76-2
benzyl 2-deoxy-5,6-O-isopropylidene-2-methylamino-β-D-glucofuranoside

: 81086-79-5
benzyl 2-(N-benzyloxycarbonyl-N-methylamino)-3-O-(D-1-carboxyethyl)-2-deoxy-5,6-O-isopropylidene-β-D-glucofuranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 0.5 M sodium carbonate / dioxane / 1.5 h / 0 °C

2: 60 percent / sodium hydride / dioxane / 2.5 h / 60 °C

With sodium hydride; sodium carbonate; In 1,4-dioxane;
DOI:10.1016/S0008-6215(00)80680-1