1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit

Base Information

Chemical Name:1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit
CAS No.:122901-09-1
Molecular Formula:C₄₆H₅₀O₉S
Molecular Weight:778.964
Hs Code.:

Synonyms:1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit

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Chemical Property of 1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit

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Technology Process of 1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit

There total 2 articles about 1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 122901-07-9
1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-muco-inosit

: 124-63-0
methanesulfonyl chloride

: 122901-09-1
1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit

Guidance literature:: With pyridine; In dichloromethane; for 15h; Ambient temperature;

Reference yield:

: 106988-98-1
1L-1,2-anhydro-3,4,5,6-tetra-O-benzyl-6-C-(benzyloxymethyl)-chiro-inosit

: 122901-09-1
1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / boron triflouride-ether / CH₂Cl₂ / 18 h / Ambient temperature

2: 98 percent / pyridine / CH₂Cl₂ / 15 h / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; In dichloromethane;

Reference yield:

: 122901-09-1
1L-2-O-allyl-1,4,5,6-tetra-O-benzyl-4-C-benzyloxymethyl-3-O-methylsulfonyl-muco-inosit

: 122901-13-7
1L-1-O-acetyl-6-azido-2,3,4,5-tetra-O-benzyl-2-C-benzyloxymethyl-6-desoxy-myo-inosit

Guidance literature:: Multi-step reaction with 4 steps

1: 1) 95percent HAc, sodium acetate, Pd(II)Cl₂ 2) allyl alcohol / 1) acetone, 15 h stirred 2) 1 h stirred

2: 80 percent / 1 M CH₃ONa / methanol; CH₂Cl₂ / 16 h / Ambient temperature

3: 88 percent / NaN₃ / dimethylformamide / 17 h / 120 °C

4: 99 percent / pyridine

With pyridine; sodium azide; sodium methylate; sodium acetate; acetic acid; allyl alcohol; palladium dichloride; In methanol; dichloromethane; N,N-dimethyl-formamide;