(+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol

Base Information

Chemical Name:(+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol
CAS No.:1188386-22-2
Molecular Formula:C₃₉H₄₆F₂O₃Si₂
Molecular Weight:656.96
Hs Code.:

Synonyms:(+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol

Suppliers and Price of (+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol

Chemical Property:

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Technology Process of (+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol

There total 1 articles about (+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₄₃H₅₂F₂O₄Si₂

: 1188386-22-2
(+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol

Guidance literature:: With methanol; pyridinium p-toluenesulfonate; at 20 ℃; for 3h;
DOI:10.1016/j.tet.2009.06.095

Reference yield: 41.0%

: 1188386-22-2
(+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol

: 4330-20-5
N-3-benzoylthymine

: 1188386-24-4
C₄₄H₅₀F₂N₂O₄Si₂

: 1119274-74-6
C₄₄H₅₀F₂N₂O₄Si₂

Guidance literature:: (+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol; N-3-benzoylthymine; With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -40 - 20 ℃;

With ammonia; In methanol; at -4 ℃; for 12h; regioselective reaction;
DOI:10.1016/j.tet.2009.06.095

Reference yield:

: 1188386-22-2
(+/-)-4,4-bis-((tert-butyldiphenylsiloxy)methyl)-5,5-difluoro-cyclopent-2-en-1-ol

: 4330-20-5
N-3-benzoylthymine

: C₅₁H₅₄F₂N₂O₅Si₂

: C₅₁H₅₄F₂N₂O₅Si₂

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at -40 - 20 ℃; regioselective reaction;
DOI:10.1016/j.tet.2009.06.095